描述
开 本: 16开纸 张: 轻型纸包 装: 平装-胶订是否套装: 否国际标准书号ISBN: 9787121359989
内容简介
本书根据高等院校工科专业学生对化学实验学习的需求及特点编写而成。本实验教材与大学普通化学课程相对应。教材分为4部分：第1部分简要介绍实验室安全、基本实验操作及数据处理；第2部分介绍10个不同的实验，这些实验分别与普通化学教学中的化学热力学、化学动力学、溶液、电化学、配位化合物等理论内容相对应；第3部分是附录，包含实验中用到的一些数据；第4部分是化学实验报告。
目 录
Content
Part 1 General Principles in Chemical Laboratory 1
Chapter 1 Chemical Laboratory Safety Rules 1
Chapter 2 General Operations 6
Chapter 3 Data and Error Analysis 12
Part 2 Experiments 15
Experiment 1 Determination of the Ideal Gas Constant 15
Experiment 2 Determination of Enthalpy of Chemical Reaction— Zn and
CuSO4 Reaction 23
Experiment 3 Chemical Reaction Rate 28
Experiment 4 Electrochemistry 36
Experiment 5 Inorganic Compound 44
Experiment 6 Determination of Dissociation Constant of Bromothymol by
Spectrophotometric Method 51
Experiment 7 Synthesis of Potassium Trioxalatoferrate(III) 63
Experiment 8 Determination of Calcium and Magnesium Ion in Water by
Complexometric Titrations with EDTA 66
Experiment 9 Determination of Mo(VI) Content by Visual Catalytic Kinetics
Method 72
Experiment 10 Separation of Coordination Compounds by Ion Exchange
Resin 78
Part 3 Appendices 83
Appendix 1 Specification and Selection of Chemical Reagent 83
Appendix 2 Density and Concentration of Commonly Used Acid or
Base Solutions (15℃) 84
Appendix 3 Color of Common Ions 85
Appendix 4 International Relative Atomic Mass 86
Appendix 5 Standard Electrode Potential 88
Appendix 6 Saturated Vapor Pressure of Water at Different Temperature 92
Appendix 7 Stability Constant of Some Coordinated Ions 94
Appendix 8 Boiling Point of Water at Different Pressure 95
Appendix 9 Density of Water at Different Temperature 96
Appendix 10 Relationship Between pH and Temperature of Buffer
Solutions 97
Appendix 11 Dissociation Constant of Some Common Weak Electrolytes
(298.15 K) 98
Appendix 12 Solubility Product of Some Common Substances 99
Appendix 13 Symbols,Values and SI Units of Some Constants 100
Part 4 Experimental Reports 101
Experimental Report 1 101
Experimental Report 2 103
Experimental Report 3 106
Experimental Report 4 110
Experimental Report 5 112
Experimental Report 6 114
Experimental Report 7 117
Experimental Report 8 119
Experimental Report 9 121
Experimental Report 10 124
Part 1 General Principles in Chemical Laboratory 1
Chapter 1 Chemical Laboratory Safety Rules 1
Chapter 2 General Operations 6
Chapter 3 Data and Error Analysis 12
Part 2 Experiments 15
Experiment 1 Determination of the Ideal Gas Constant 15
Experiment 2 Determination of Enthalpy of Chemical Reaction— Zn and
CuSO4 Reaction 23
Experiment 3 Chemical Reaction Rate 28
Experiment 4 Electrochemistry 36
Experiment 5 Inorganic Compound 44
Experiment 6 Determination of Dissociation Constant of Bromothymol by
Spectrophotometric Method 51
Experiment 7 Synthesis of Potassium Trioxalatoferrate(III) 63
Experiment 8 Determination of Calcium and Magnesium Ion in Water by
Complexometric Titrations with EDTA 66
Experiment 9 Determination of Mo(VI) Content by Visual Catalytic Kinetics
Method 72
Experiment 10 Separation of Coordination Compounds by Ion Exchange
Resin 78
Part 3 Appendices 83
Appendix 1 Specification and Selection of Chemical Reagent 83
Appendix 2 Density and Concentration of Commonly Used Acid or
Base Solutions (15℃) 84
Appendix 3 Color of Common Ions 85
Appendix 4 International Relative Atomic Mass 86
Appendix 5 Standard Electrode Potential 88
Appendix 6 Saturated Vapor Pressure of Water at Different Temperature 92
Appendix 7 Stability Constant of Some Coordinated Ions 94
Appendix 8 Boiling Point of Water at Different Pressure 95
Appendix 9 Density of Water at Different Temperature 96
Appendix 10 Relationship Between pH and Temperature of Buffer
Solutions 97
Appendix 11 Dissociation Constant of Some Common Weak Electrolytes
(298.15 K) 98
Appendix 12 Solubility Product of Some Common Substances 99
Appendix 13 Symbols,Values and SI Units of Some Constants 100
Part 4 Experimental Reports 101
Experimental Report 1 101
Experimental Report 2 103
Experimental Report 3 106
Experimental Report 4 110
Experimental Report 5 112
Experimental Report 6 114
Experimental Report 7 117
Experimental Report 8 119
Experimental Report 9 121
Experimental Report 10 124
前 言
Preface
General chemistry and general chemistry experiments are important curriculum in an engineering university for students majoring in engineering and chemistry related. The general chemistry experiment course aims to further verify the fundamental principles of chemistry showing in general chemistry class, training professional skills by practice, provides a good link between theory and practice in general chemistry, and cultivate scientific approach in seeking the truth from facts. Through this course, students can finally improve their ability of practice, observe and analysis when face to problems in further study and daily lives.
This book was designed to help students majoring in engineering or biology to find their special interests in chemistry experiments as non-professional chemists. This book includes 10 experiments. This book includes 10 experiments. Dr. Wangchang Geng provided the writing outlines and requirements. Experiments 1~3 were edited by Dr. Fang Chen, Experiments 1~3 were edited by Dr. Fang Chen, Experiments 4~6 were edited by Dr. Wangchang Geng, Experiments 7~10 were edited by Dr. Jing Yan Dr. Jing yan. Dr. Xin Wang was responsible for the correction of this text book. Authors would like thank these teachers from the Teaching and Research Group of General Chemistry in NPU for their generous help with the preparation of this book.
Your comments or feedback about this book are most welcome.
Wang chang Geng Jing Yan Fang Chen Xin Wang
General chemistry and general chemistry experiments are important curriculum in an engineering university for students majoring in engineering and chemistry related. The general chemistry experiment course aims to further verify the fundamental principles of chemistry showing in general chemistry class, training professional skills by practice, provides a good link between theory and practice in general chemistry, and cultivate scientific approach in seeking the truth from facts. Through this course, students can finally improve their ability of practice, observe and analysis when face to problems in further study and daily lives.
This book was designed to help students majoring in engineering or biology to find their special interests in chemistry experiments as non-professional chemists. This book includes 10 experiments. This book includes 10 experiments. Dr. Wangchang Geng provided the writing outlines and requirements. Experiments 1~3 were edited by Dr. Fang Chen, Experiments 1~3 were edited by Dr. Fang Chen, Experiments 4~6 were edited by Dr. Wangchang Geng, Experiments 7~10 were edited by Dr. Jing Yan Dr. Jing yan. Dr. Xin Wang was responsible for the correction of this text book. Authors would like thank these teachers from the Teaching and Research Group of General Chemistry in NPU for their generous help with the preparation of this book.
Your comments or feedback about this book are most welcome.
Wang chang Geng Jing Yan Fang Chen Xin Wang
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