描述
开 本: 16开纸 张: 胶版纸包 装: 平装-胶订是否套装: 否国际标准书号ISBN: 9787564367893
本书内容主要涉及聚合物的形态结构、高分子溶液的性质、聚合物的力学性能、聚合物的热性能、聚合物的加工性能、聚合物的电性能以及聚合物乳液的性质等方面，共精选了20个实验，都是合成与加工中需要做的一些测试方法和手段。每个实验都介绍与实验有关的基本原理和明确的目的要求、实验步骤、仪器和药品、数据处理以及需要思考的问题等；书后附有12个附表，方便查阅。本书充分体现了重庆文理学院高分子物理实验教学的特色，体现了作者近年的教学研究成果与科研成果。
目 录
单元 聚合物的溶液性质································································································ 1
实验一 聚合物的逐步沉淀分级法··················································································· 1
实验二 黏度法测定聚合物分子量··················································································· 6
实验三 聚合物的溶解································································································· 10
实验四 聚合物表面的接触角测定················································································· 14
第二单元 聚合物的结构分析······························································································· 17
实验五 溶胀平衡法测定聚合物的交联度······································································· 17
实验六 偏光显微镜法观察聚合物球晶··········································································· 22
实验七 结晶速率仪测定聚合物的结晶速率···································································· 25
实验八 红外光谱法鉴定聚合物···················································································· 29
实验九 偏光显微镜法观察聚合物球晶形态···································································· 32
第三单元 聚合物的热性能·································································································· 38
实验十 转矩流变仪测聚氯乙烯热稳定性······································································· 38
实验十一 差示扫描量热法（DSC）测定聚合物的热性能················································· 43
实验十二 热重法（TG）测定聚合物热降解反应动力学参数············································ 47
实验十三 聚合物耐热性能的测试················································································· 54
第四单元 聚合物的力学性能······························································································· 58
实验十四 聚合物冲击性能的测试················································································· 58
实验十五 聚合物拉伸性能的测试················································································· 62
实验十六 聚合物硬度的测试························································································ 65
第五单元 聚合物的加工性能······························································································· 68
实验十七 热塑性塑料聚氯乙烯的塑化、力学性能试样压制、成型实验····························· 68
实验十八 热塑性塑料的挤出造粒与注塑成型································································· 73
第六单元 聚合物熔体的其他性质（熔体流动特性、电性能）················································· 83
实验十九 高聚物熔体流动特性的测试··········································································· 83
实验二十 高阻仪测定聚合物的电阻·············································································· 87
附 表······························································································································· 94
主要参考文献··················································································································· 105
前 言
高分子物理实验是高分子材料与工程专业本科学生必修的专业实验课程。高分子物理实验的教学目的和目标，是让学生了解高分子材料常用测试方法的测试原理以及仪器结构，掌握高分子材料的研究方法，提高学生的动手能力，扩大学生的知识面，培养学生获取知识、提出问题、分析问题的能力，并使学生具有一定的创新意识和创新能力。
本书的内容主要涉及聚合物的形态结构、高分子溶液的性质、聚合物的力学性能、聚合物的热性能、聚合物的加工性能以及聚合物的电性能等方面，共精选了20个实验，都是高分子材料性能测试及加工过程中需要掌握的常规测试方法和手段。书中对每一个实验的目的、基本原理都做了较详细的叙述；对实验技术的关键问题，实验过程中需特别注意的事项等均注以详细的说明和图解。每个实验后面均列有思考题，便于读者加深对实验的理解和掌握。
本书主要根据应用型教材教学大纲和对学生实验的要求进行编写。在实验水平上，既介绍高分子科学的传统实验方法，也尽可能介绍一些有关的新技术。对近年来高分子科学，特别是高分子物理领域涌现的许多新方法、新技术，我们也有相应的引进。本书可作为本科院校高分子专业学生及老师的参考书，也可供从事高分子科学和材料研制、开发、测试的科技人员阅读。
由于作者水平有限，书中难免存在不足之处，敬请读者批评指正
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